Analytical Chemistry Advanced 310-CS2-1CANZ

general academic profile, full-time studies, compulsory subject; field: exact and natural sciences; discipline: chemical sciences;
Year of studies/semester: 1st year/2nd cycle/1st semester; number of teaching hours divided into forms of classes: lecture - 25 hours, laboratory -30 hours; teaching methods: multimedia presentation (lecture), chemical experiment (laboratory); 3 ECTS;
Total student workload:75 hours, including participation in lectures: 25 hours, participation in laboratory classes: 30 hours; non-lectures preparation for classes and tests: 41.3 hours; participation in consultations, tests: 3.8 hours;

Quantitative indicators: total student workload related to classes: 75 hours, including requiring direct teacher participation: 33.8 hours; practical: 50.0 hours.

Term 2024:

The importance of analytical chemistry, the role of analytical tools. The analytical process and the characteristics of its individual stages. Basic concepts related to it: sample, signal, measurement principle (analytical technique), analytical method, analytical procedure. Compositional, distribution, structural, process analytics. The concept of trace analysis and its specificity. Errors in chemical analysis and the causes of their occurrence. Principles and methods of sampling. Sampling of solid materials, samplers for taking solid samples. Techniques for reducing a solid sample. Sampling of loose, lumpy samples, soil, plant materials, sediments. Sampling of gaseous and liquid materials. Methods of storing and transporting solid, liquid and gaseous samples. Documenting the sampling stage, control of the sample preparation process. Typical operations of the sample preparation stage for analysis. Methods of digesting inorganic and organic samples. Methods of separating and concentrating analytes, eliminating interfering substances and matrix effects. Calibration of analytical methods. Validation of analytical methods – parameters of the validation process. Latest achievements and directions of development in analytical chemistry: green analytical chemistry; miniaturization in sample preparation for analysis; miniature chemical sensors; flow and coupled techniques; multifunctional molecular materials in chemical analysis; porous, magnetic and nanomaterials; speciation and speciation analysis.

Term 2025:

Term 2026:

Course coordinators

Beata Godlewska-Żyłkiewicz

Type of course

obligatory courses

Mode

(in Polish) w sali

Learning outcomes

Knowledge:
Students gain advanced knowledge of chemistry and deepens their understanding of analytical chemistry. They define key concepts in analytical chemistry, including analytical process, sample, analyte, measurement principle, analytical method, and analytical procedure. They understand methods for collecting and preparing various types of samples for analysis. They understand the concept of trace analysis and its specificity. They are familiar with the latest trends in analytical chemistry, including the requirements of green analytical chemistry, sensors: types and applications, the concepts of speciation and speciation analysis, multifunctional molecular materials and their areas of application. They understand the properties and methods of determining chemical elements and compounds based on their advanced knowledge of analytical chemistry KP7_WG1, KP7_WG2

Skills:
Students can select the appropriate method for analyte collection, preparation, and determination to solve a given analytical problem. They can plan the analytical process, utilize the principles of green chemistry in experimental planning. The students can analyze research results, apply statistical methods and computer techniques to analyze experimental data, and critically analyze and identify measurement errors and their causes. They can justify the purpose of the research and its significance in comparison to similar studies. They can identify relevant legal regulations governing the content of analytes in various products. KP7_UW6

Competencies:
The student is willing to work in a team, assuming various roles, verifies and respects the opinions of other team members, and is responsible for the safety of their own work and that of others. The student demonstrates a willingness to independently expand their knowledge of analytical chemistry by searching for information in specialized literature, databases, and legal acts. KP7_KO2

Assessment criteria

Course assessment methods: lecture – written examination, with a passing grade required for the written examination; laboratory – attendance, completion of all exercises, and submission of written reports, with a grade.

Assessment criteria are consistent with the principles set forth in the University of Białystok Study Regulations, adopted by Resolution No. 2527 of the University of Białystok Senate on June 26, 2019.
Flexible forms of assessment may be introduced in consultation with the lecturer and student, but such terms should be established at the beginning of the teaching cycle. The scope and manner of using AI tools are specified in the Order of the Rector of the University of Bialystok on the use of Artificial Intelligence systems in the educational process at the University of Bialystok.

Bibliography

Literatura podstawowa:
1. Skoog D. A., West D. M., Holler F .J., Crouch S. R., Podstawy chemii analitycznej cz. 3, Wydawnictwo Naukowe PWN, Warszawa, 2024. (wybrane rozdziały)
2. Hulanicki A., Współczesna chemia analityczna. Wybrane zagadnienia. Wydawnictwo Naukowe PWN, Warszawa, 2022.
3. Baranowska I. (red.), Analiza śladowa. Zastosowania. Wydawnictwo MALAMUT, Warszawa, 2013.(wybrane rozdziały)
4. E.H.Evans, M.E. Foulkes, Chemia analityczna podejście praktyczne, PWN 2020.
5. 5. Stepnowski P., Synak E., Szafranek B., Kaczyński Z., Techniki separacyjne (rozdziały: „Ekstrakcja w układzie ciecz-ciało stałe” oraz „Połączenie chromatografii ze spektrometrią mas”), Wydawnictwo UG, Gdańsk 2010 (dostępne online).

Literatura uzupełniająca:
1. Jarosz M. (red.), Nowoczesne techniki analityczne. Oficyna Wydawnicza Politechniki Warszawskiej, Warszawa.
2. Brzózka Z. 2009. Mikrobioanalityka, Oficyna Wydawnicza Politechniki Warszawskiej, Warszawa, 2006.
3. Barałkiewicz D., Bulska E. (red.), Specjacja chemiczna. Problemy i możliwości. Wydawnictwo MALAMUT, Warszawa, 2009.
4. Żyrnicki W., Borkowska-Borecka J., Bulska E., Szmyd E. (red.), Metody analitycznej spektrometrii atomowej. Teoria i praktyka. Wydawnictwo MALAMUT, Warszawa, 2010.
5. Namieśnik J., Łukasiak J. Jamrógiewicz Z., Pobieranie próbek środowiskowych do analizy, PWN, Warszawa, 1995.
6. Namieśnik J., Jamrógiewicz Z., Pilarczyk M., Torres L., Przygotowanie próbek środowiskowych do analizy, WNT, Warszawa, 2000.
7. Konieczka P., Namieśnik J., Ocena i kontrola jakości wyników pomiarów analitycznych. WNT, Warszawa, 2007.

Term 2024:

Term 2025:

Term 2026:

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 310-CS2-1CANZ in USOSweb