(in Polish) Advanced Analytical Chemistry 310-ERS-CAZE

general profile, full-time studies, obligatory subject; field: sciences and natural sciences; discipline: chemical sciences;

Year of studies/semester: 1st year/ 2nd degree/I semester; number of hours of teaching divided into forms of teaching: lecture - 25 hours, laboratory - 30 hours; teaching methods: multimedia presentation (lecture), chemical experiment (laboratory); 4 ECTS;

Total student workload: 100 hours, including participation in lectures: 25 hrs, participation in laboratory classes: 30 hrs; preparation for classes and credits: 38.1 hrs; participation in consultations, credits: 6.9 hrs;

Quantitative indicators: total student workload related to classes: 100 hours, including those requiring direct participation of the teacher: 61.9 hours; of a practical nature: 75.0 hrs.

Term 2024:

Lecture 1. The importance of analytical chemistry, the role of analytical tools. the importance of analytical information. Characteristics of the basic concepts of the elements of the analytical process: sample, signal, analytical method, analytical procedure. Composition, distribution, structural and process analytics. Multidimentional techniques in chemical analysis. Role of chemometrics in analytical chemistry. The concept of trace analysis and its specificity. Steps of analytical process and analytical procedure. Criteria for proper selection of analytical methods.
Lecture 2. Chemical analysis errors, sources and methods of elimination.
Lecture 3. Principles and methods of sampling. Sampling of solids, samplers for collecting solid samples. Techniques for reducing a solid sample. Sampling of loose, lumpy soil, plant materials, bottom sediments. Sampling of liquids, samplers for collecting liquid samples. Samples preservation and storage.
Lectures 4. Methods for digestion of samples: extraction, leaching, decomposition, combustion, mineralisation, UV digestion for organic and inorganic samples. Dry and wet methods in open and closed systems.
Lecture 5. Introduction to sample preparation techniques. Objectives of sample preparation methods. Classification of methods. Typical operations at the stage of sample preparation for analysis.The latest achievements and directions of development of analytical chemistry
Lecture 6. Sampling and sample pretreatment methods for analysis of volatile analytes.
Lecture 7. Modern techniques for pretreatment of gaseous and solid samples (head space analysis, SPME, derivatization, ect.).
Lectures 8-9. Modern techniques for pretreatment of liquid and solid samples - liquid-liquid extraction, ect. . Miniarurisation of LLE methods.
Lecture 10. Modern solid phase extraction technique: multifunctional molecular materials in chemical analysis; porous, magnetic and nanomaterials.
Lectures 11. Miniaturisation in chemical analysis. Principles and applications of flow analytical techniques.
Lecture 12. Speciation and speciation analysis.

Term 2025:

Term 2026:

Type of course

obligatory courses

Course coordinators

Term 2024:

Edyta Nalewajko-Sieliwoniuk

Term 2025:

Edyta Nalewajko-Sieliwoniuk

Term 2026:

Edyta Nalewajko-Sieliwoniuk

Term 2023:

Beata Godlewska-Żyłkiewicz

Learning outcomes

Knowledge:
The student is familiar with advanced topics in chemistry and deepens their knowledge of analytical chemistry. They define key concepts in analytical chemistry, including the analytical process, sample, analyte, measurement principle, analytical method, and analytical procedure. The student is familiar with methods of collecting and preparing various types of samples for analysis. They are familiar with the concept of trace analysis and its specific characteristics. They are familiar with the latest trends in the development of analytical chemistry, including the requirements of green analytical chemistry, sensors: types and applications, the concepts of speciation and speciation analysis, multifunctional molecular materials and their areas of application. They are familiar with the properties and methods of determining elements and chemical compounds based on their extended knowledge of analytical chemistry, (KP7_WG1, KP7_WG2).

Skills:
The student is able to select the appropriate method of sampling, preparation, and determination of the analyte to solve a given analytical problem. They are able to plan the analytical process. They are able to apply the principles of green chemistry in planning experiments. They are able to compile research results, apply statistical methods and IT techniques to analyze experimental data, and perform critical analysis and identify measurement errors and their causes. Justifies the purpose of the research and its significance in the context of similar studies. Is able to find the relevant legal regulations governing the content of the substances being determined in various types of samples. (KP7_UW6)

Competencies:
The student is ready to work in a team, taking on various roles, verifying and respecting the opinions of other team members, and is responsible for the safety of their own work and that of others. The student demonstrates a willingness to independently expand their knowledge of analytical chemistry by searching for information in specialist literature, databases, and legal acts. (KP7_KO2)

Assessment criteria

Lecture: exam in written or oral form,
laboratory: e.g., attendance in class, performance of all exercises provided for in the program, submission of written reports and theoretical credit for all exercises provided for in the program in oral or written form.

Bibliography

Literature available from the person conducting the course.

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 310-ERS-CAZE in USOSweb