Separation and Hyphenated Techniques in Chemical Analysis 310-ERS-1PDWII-14
Profile: general academic,
Study format: full-time,
Subject type: specialization;
Field and discipline: exact and natural sciences, chemical sciences,
Year of study/semester: 1st year of second-cycle studies, summer semester,
Entry requirements: none
Number of teaching hours by format: 30 hours (lecture - 15 hours, laboratory - 15 hours);
Teaching methods: expository method (lecture with multimedia presentation), chemical experiment (laboratory);
ECTS credits: 2
Quantitative indicators:
Total student workload related to classes: 50 hours,
Student workload related to classes requiring direct teacher participation: 32 hours, including participation in lectures (15 hours), participation in extra-lecture activities (15 hours), and participation in consultations/assessments/exams (2 hours).
Preparation for classes/tests/exams (student's own work): 18 hours.
Rodzaj przedmiotu
Koordynatorzy przedmiotu
Efekty kształcenia
KNOWLEDGE, student knows and understands:
- advanced topics related to modern methods of analyte separation (e.g., DLLME and its modifications, USAEME) and deepens their knowledge of separation and hyphenated techniques (KP7_WG1),
- modern measurement techniques used in hyphenated techniques based on chromatographic separation, including HPLC-ICP-MS, HPLC-AAS, HPLC-ICP-OES, EC-ICP-MS, LC-MS/MS, multidimensional chromatographic techniques (LCxLC-MS, GCxGC-MS), hyphenated techniques using electrophoresis and those based on infrared spectroscopy, and explains the theoretical basis of measurement equipment used in hyphenated techniques (KP7_WG5).
SKILLS, student is able to:
- apply acquired knowledge in the field of combining separation and identification techniques to determine biologically active compounds and metal speciation in food, environmental, and biological samples (KP7_UW4),
- analyze research results obtained using methods such as ICP-MS, GC-MS, and LC-MS/MS, utilize statistical methods and computer science techniques to analyze experimental data, critically analyze and identify potential sources of measurement error, and justify the purpose of the research and its significance in the context of other research (KP7_UW6).
SOCIAL COMPETENCES, student is ready to:
- critically review content appearing in the media, particularly in the field of separation, combined, and hybrid techniques, and understand the need for systematically reviewing the literature on the use of combined techniques in chemical analysis (KP7_KK1).
Method of verifying the achieved learning outcomes: knowledge test after completing the exercise, assessment of progress during classes, assessment of reports on completed exercises.
Kryteria oceniania
Course assessment methods: lecture – written assessment with a grade; laboratory – written assessment with a grade.
Grading criteria are consistent with the principles set forth in the University of Białystok Study Regulations, adopted by Resolution No. 2527 of the University of Białystok Senate of June 26, 2019.
For this course, the use of AI systems is prohibited during written examinations and in the preparation of laboratory reports, with the exception of: language and stylistic correction of the text,and machine translation of text from or into a foreign language.
Literatura
Basic literature:
1. Elsa Lundanes, Leon Reubsaet, Tyge Greibrokk, Chromatography: Basic Principles, Sample Preparations and Related Methods Wiley, 2013.
2. Rudolf Bock, Reinhard Nießner, Separation Techniques in Analytical Chemistry, Walter de Gruyter GmbH & Co KG, 2023.
Więcej informacji
Dodatkowe informacje (np. o kalendarzu rejestracji, prowadzących zajęcia, lokalizacji i terminach zajęć) mogą być dostępne w serwisie USOSweb: