NMR, IR and MS in Chemical Analysis 310-ERS-1PDWII-23
Profile of studies: general academic
Form of study: full-time
Type of course: Elective subject from block II – specialization
Field and discipline of science: Field of exact and natural sciences, chemical sciences
Year of study/semester: I year semester 2
Entrance requirements: Credit in the 1st semester of classes: Advanced organic chemistry and Spectroscopy.
Number of hours of classes divided into forms of teaching: Lecture 15 hours and laboratory 15 hours. Teaching methods: Lecture with elements activating students (in the lecture hall or online), laboratory (in the classroom or remotely - independent implementation of tasks).
ECTS points: 2
Student's workload balance: Hours/ECTS
Total student workload related to classes: 50/2
Student's workload related to classes requiring direct participation of the teacher: 32/1.3 including:
1) participation in lectures: 15/0.6
2) participation in extracurricular activities: 15/0.6
3) participation in consultations/credits/exams: 2/0.1
Preparation for classes/credits/exams (student's own work): 18/0.7% of student's own working hours: 36%
Rodzaj przedmiotu
fakultatywne specjalizacyjne
Założenia (opisowo)
Koordynatorzy przedmiotu
Efekty kształcenia
KP7_WG5 - learns about modern measurement techniques used in chemical analysis, such as mass spectrometry (MS), IR spectroscopy (FTIR) and NMR spectroscopy. He/she can explain the theoretical basis of the MS spectrometer and the IR and NMR spectroscope with Fourier transform.
KP7_UW4 - can use the acquired chemical knowledge to analyse data obtained from MS, IR and NMR. He/she can interpret the obtained measurement results and uses them in solving in the field of chemistry and related fields such as biology, environmental protection, pharmacy and medicine
KP7_UW6 - can develop the results of measurements obtained by MS, IR and NMR methods. In data analysis, he/she can use statistical methods and IT techniques provided for the analysis of experimental data. He/she can analyse the results obtained (spectra) and can critically assess the quality of measurement and indicate measurement errors. He/she can justify the necessity or non-need for spectroscopic tests and is able to compare their importance with other tests used in laboratory work.
KP7_KK1 – He/she can critically assess information provided in the media, e.g. the harmfulness of IR or NMR measurements. He/she understands the need to systematically familiarize himself with professional literature, new technical solutions in the field of MS, IR and NMR methods.
Kryteria oceniania
Teaching methods:
Activating lecture (15 hours) as part of the lectures (conversational lecture) discussion, creating problem groups, multimedia presentations.
Exercises (15 hours) – problem work in groups, evaluation of the effects of teamwork (reports) and individual work during classes.
Assessment criteria:
1. Completion of the course (lecture and exercises) takes place in writing and on the basis of attendance at classes.
2. The condition for passing the exam is: - obtaining at least 51% of the possible points from each exercise and from the written tests as part of the lecture.
3. An unexcused absence of a student from more than three classes (lectures plus classes) qualifies for failure of the course. In the case of excused absence from the lecture, the student is obliged to master the material on his/her own and, if necessary, prepare answers to the issues sent by the lecturer. However, the method of making up for exercises must be agreed individually with the person conducting classes in accordance with the Study Regulations.
5.5. The assessment is made on the basis of assessment criteria in accordance with the Study Regulations: (https://chemia.uwb.edu.pl/studenci)
Literatura
T.N. Mitchell, B. Costisella „NMR – From Spectra to Structures” Springer 2007
Y-C. Ning „Structural Identification of Organic Compounds with Spectroscopic Techniques” Wiley-VCH 2005
E. Breitmaier „Structure Elucidation by NMR in Organic Chemistry” Wiley 2007
R. Silverstein, F.Webster, D. Kiemle, Spectrometric Identification of Organic Compounds
NMR - From Spectra to Structures - An Experimental Approach - 2nd Edition – 2007 "Organic Spectroscopy" - online lectures by Prof. James S. Nowick (Department of Chemistry, University of California)
Więcej informacji
Dodatkowe informacje (np. o kalendarzu rejestracji, prowadzących zajęcia, lokalizacji i terminach zajęć) mogą być dostępne w serwisie USOSweb: