Physicochemical Methods of Analysis 310-ERS-1PDWII-31
Profile of education: Academic (A)
Lecture language: English
Form of classes: lecture - 30 hours, laboratory classes - 45 hours
Student activity form:
Summary student workload: 175 h
Participation in lectures : 30 h
Participation in laboratories: 45
Preparation for classes, tests, presentation and exam: 90.6 h
Tests, presentation, exam, consultations: 9.4 h
Total student workload related to classes:
1) requiring direct teacher participation: 84.4 h, ECTS credits 3.4
2) of a practical nature 145 h ECTS credits 5.8
Module ECTS credits: 7
Lecture topics: Conductivity, potentiometry, spectrophotometry, adsorption isotherms, chronoamperometry, stripping voltammetry, chronopotentiometry, electrolysis, electrocoagulation, electroflotation, electrooxidation, application of microelectrodes, alternating current and pulse voltammetry, spectroelectrochemistry, lithium ion batteries.
Laboratory exercises.
1. Quantitative determination of lead by the conductometric titration method
2. Potentiometry, Ion-selective electrodes
3. Spectrophotometric determination of the adsorption isotherm of methylene blue on carbon.
4. Chronoamperometry
5. Stripping voltammetry
6. Chronopotentiometry
7. Removal of arsenic form water by electrocoagulation. Determination of the process efficiency using stripping voltammetry on a gold microelectrode.
8. Analytical application of alternating current and pulse voltammetry
9. Spectroelectrochemistry
10. Lithium Batteries
Didactic methods:
lecture: giving method (traditional lecture, conversation lecture, lecture with elements of student activation, problem method) project method, work with text, demonstration method, student presentation, calculus exercises,
laboratory: e.g. practical exercises, experiment, observation.
The subject is implemented in the form of a lecture combined with a seminar and laboratory exercises. As part of the lecture, students are given sample physicochemical problems to solve, which are then discussed in lecture and during consultations.
Rodzaj przedmiotu
Koordynatorzy przedmiotu
Efekty kształcenia
Knowledge,
KP7_WG1, Student knows and understands the basic concepts of physical chemistry, thermodynamics, electrochemistry, phase equilibria, chemical kinetics, photochemistry and describes their relationship with other fields of science,
KP7_WG5, Student knows and understands modern measurement techniques used in chemical analysis, explains the theoretical basis of the operation of measuring equipment used in chemical research;
Abilities,
KP7_UW3, Student is able to use specialist literature, databases and other sources to obtain necessary information and knows basic national and international scientific journals in the field of chemistry,
KP7_UW4, Student is able to apply acquired chemical knowledge to analyze problems in chemistry and related fields such as biology, environmental protection, pharmacy, medicine
KP7_UW6, Student is able to process research results, applies statistical methods and IT techniques to analyze experimental data and performs a critical analysis and indicates measurement errors, justifies the purpose of the research and its importance against the background of similar research;
Social competences,
KP7_KK1, Student is ready to critically evaluate the information disseminated in the media, especially in the field of chemistry, understands the need for systematic reading of professional literature.
Methods of verifying learning outcomes: Written exam, assessment of activity during classes, assessment of reports and tests, assessment of independently prepared presentation.
Kryteria oceniania
Compulsory classes, absences must be made up for. Written credit, proper execution of the exercise, active participation in classes, assessment of the laboratory reports.
Final grade = 0.2 grade from presentation + 0.8 grade from examination.
Grading criteria:
A - at least 91% of points,
B - at least 81% of points,
C - at least 71% of points,
D - at least 61% of points,
E - at least 51% of points.
It is possible to introduce flexible forms of credit in agreement between the lecturer and the student in accordance with the principles of universal design, with such conditions to be established at the beginning of the teaching cycle.
Literatura
1. P. Atkins and J. De Paula Atkins’ Physical Chemistry, Oxford University Press, 2006
2. D.C. Harris, “Quantitative Chemical Analysis”,
3. J. Wang, “ Analytical Electrochemistry”
4. A.J. Bard and L.R. Faulkner, “Electrochemical Methods Fundamentals and applications”
5. V.S. Bagotsky, “Fundamentals of electrochemistry”
6. F.W.Fifield and D. Kealey, “Principles and practice of analytical chemistry”
7. D. Harvey, “ Modern Analytical Chemistry”
8. D. A. Skoog, “Principles of Instrumental Analysis”
9. P.V. Nidheesh , T.S. Anantha Singh, Arsenic removal by electrocoagulation process: Recent trends and removal mechanism, Chemosphere 181 (2017) 418e432
10. Karel Štulík, Christian Amatore, Karel Holub, Vladimír Mareček, and Włodzimierz Kutner, Microelectrodes. definitions, characterization and applications, Pure Appl. Chem., Vol. 72, No. 8, pp. 1483–1492, 2000
Więcej informacji
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