Physicochemical Methods of Analysis 310-ERS-1PDWII-31
Profile of education: Academic (A)
Lecture language: English
Form of classes: lecture - 30 hours, laboratory classes - 60 hours
Student activity form:
Summary student workload: 200 h
Participation in lectures and laboratories: 90 h
Preparation of presentation: 30 h
Preparation for classes, tests and exam: 68 h
Module ECTS credits: 8
Lecture topics: Conductivity, potentiometry, spectrophotometry, adsorption isotherms, chronoamperometry, stripping voltammetry, chronopotentiometry, electrolysis, electrocoagulation, electroflotation, electrooxidation, application of microelectrodes, alternating current and pulse voltammetry, spectroelectrochemistry, lithium ion batteries.
Laboratory exercises.
1. Quantitative determination of lead by the conductometric titration method
2. Potentiometry, Ion-selective electrodes
3. Spectrophotometric determination of the adsorption isotherm of methylene blue on carbon.
4. Chronoamperometry
5. Stripping voltammetry
6. Chronopotentiometry
7. Removal of arsenic form water by electrocoagulation. Determination of the process efficiency using stripping voltammetry on a gold microelectrode.
8. Analytical application of alternating current and pulse voltammetry
9. Spectroelectrochemistry
10. Lithium Batteries
Rodzaj przedmiotu
Koordynatorzy przedmiotu
Efekty kształcenia
Student knows and understands the basic concepts of physical chemistry, thermodynamics, electrochemistry, phase equilibria, chemical kinetics, photochemistry and describes their relationship with other fields of science
Student is able to: identify and solve chemical problems based on the acquired knowledge, learn independently selected issues, independently plan and implement their own lifelong learning in order to improve their own competences
Student is ready to critically evaluate the information disseminated in the media, especially in the field of chemistry
Student knows and understands modern measurement techniques used in chemical analysis, explains the theoretical basis of the operation of measuring equipment used in chemical research;
Student is able to process research results, applies statistical methods and IT techniques to analyze experimental data and performs a critical analysis and indicates measurement errors, justifies the purpose of the research and its importance against the background of similar research;
student is ready to work in a team, assuming various roles in it, verifies and respects the opinion of other team members, is responsible for the safety of his own and others' work.
Kryteria oceniania
Compulsory classes, absences must be made up for. Written credit, proper execution of the exercise, active participation in classes, assessment of the laboratory reports.
Final grade = 0.3 grade from laboratory classes + 0.2 grade from presentation + 0.5 grade from examination
to obtain a rating A must be obtained at least 91% of points, to obtain rating B at least 81% of points, the C rating at least 71% of points,
the rating D at least 61% of points D and rating E at least 51% of points.
Literatura
1. P. Atkins and J. De Paula Atkins’ Physical Chemistry, Oxford University Press, 2006
2. D.C. Harris, “Quantitative Chemical Analysis”,
3. J. Wang, “ Analytical Electrochemistry”
4. A.J. Bard and L.R. Faulkner, “Electrochemical Methods Fundamentals and applications”
5. V.S. Bagotsky, “Fundamentals of electrochemistry”
6. F.W.Fifield and D. Kealey, “Principles and practice of analytical chemistry”
7. D. Harvey, “ Modern Analytical Chemistry”
8. D. A. Skoog, “Principles of Instrumental Analysis”
9. P.V. Nidheesh , T.S. Anantha Singh, Arsenic removal by electrocoagulation process: Recent trends and removal mechanism, Chemosphere 181 (2017) 418e432
10. Karel Štulík, Christian Amatore, Karel Holub, Vladimír Mareček, and Włodzimierz Kutner, Microelectrodes. definitions, characterization and applications, Pure Appl. Chem., Vol. 72, No. 8, pp. 1483–1492, 2000
Więcej informacji
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