(in Polish) Advanced Analytical Chemistry 310-ERS-CAZE

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Term 2024:

Lecture 1. The importance of analytical chemistry, the role of analytical tools. the importance of analytical information. Characteristics of the basic concepts of the elements of the analytical process: sample, signal, analytical method, analytical procedure. Composition, distribution, structural and process analytics. Multidimentional techniques in chemical analysis. Role of chemometrics in analytical chemistry. The concept of trace analysis and its specificity. Steps of analytical process and analytical procedure. Criteria for proper selection of analytical methods.
Lecture 2. Chemical analysis errors, sources and methods of elimination.
Lecture 3. Principles and methods of sampling. Sampling of solids, samplers for collecting solid samples. Techniques for reducing a solid sample. Sampling of loose, lumpy soil, plant materials, bottom sediments. Sampling of liquids, samplers for collecting liquid samples. Samples preservation and storage.
Lectures 4. Methods for digestion of samples: extraction, leaching, decomposition, combustion, mineralisation, UV digestion for organic and inorganic samples. Dry and wet methods in open and closed systems.
Lecture 5. Introduction to sample preparation techniques. Objectives of sample preparation methods. Classification of methods. Typical operations at the stage of sample preparation for analysis.The latest achievements and directions of development of analytical chemistry
Lecture 6. Sampling and sample pretreatment methods for analysis of volatile analytes.
Lecture 7. Modern techniques for pretreatment of gaseous and solid samples (head space analysis, SPME, derivatization, ect.).
Lectures 8-9. Modern techniques for pretreatment of liquid and solid samples - liquid-liquid extraction, ect. . Miniarurisation of LLE methods.
Lecture 10. Modern solid phase extraction technique: multifunctional molecular materials in chemical analysis; porous, magnetic and nanomaterials.
Lectures 11. Miniaturisation in chemical analysis. Principles and applications of flow analytical techniques.
Lecture 12. Speciation and speciation analysis.

Type of course

obligatory courses

Course coordinators

Beata Godlewska-Żyłkiewicz

Learning outcomes

The student knows and understands:
- issues concerning an advanced chemistry and deep their knowledge in the selected specialization (KP7_WG1),
- structure, properties and methods of obtaining chemical compounds based on the extended knowledge in a scope of chemistry (KP7_WG2).

The student is able to:
- develop research results, apply statistical methods and IT techniques to analyze experimental data and perform a critical analysis and indicate measurement errors, justify the purpose of the research and their importance in comparison with similar studies (KP7_UW6),
- working in a team by assuming different roles in it, verifying and respecting the opinion of other team members, is responsible for the safety of his own work and that of others (KP7_KO2).

Assessment criteria

Ways of verifying the learning outcomes: tests, evaluation of exercises and reports, exam.

The condition for obtaining credit is the attendance at the classes and completion of all the analyzes provided for in the program.

Bibliography

Literature available from the person conducting the course.

Additional information

Additional information (registration calendar, class conductors, localization and schedules of classes), might be available in the USOSweb system:

Description of 310-ERS-CAZE in USOSweb